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Ultra High Vacuum Degassing Chamber
  • Ultra High Vacuum Degassing Chamber
  • Ultra High Vacuum Degassing Chamber
  • Ultra High Vacuum Degassing Chamber
  • Ultra High Vacuum Degassing Chamber
  • Ultra High Vacuum Degassing Chamber
Ultra High Vacuum Degassing ChamberUltra High Vacuum Degassing ChamberUltra High Vacuum Degassing ChamberUltra High Vacuum Degassing ChamberUltra High Vacuum Degassing Chamber

Ultra High Vacuum Degassing Chamber

Ultra High Vacuum (UHV) Degassing Chambers operate at extreme vacuum levels (typically 10-9 to 10-12 torr) and are engineered to remove trace contaminants, adsorbed gases, and volatile compounds from materials or components. Their applications span industries where atomic-scale cleanliness and material stability are mission-critical

The complete system comprises the vacuum vessel, the vacuum pumping subsystem, the thermal subsystem and the control subsystem.

Product Details

 1. Semiconductor & Quantum Device Fabrication

Wafer Processing: Removes hydrocarbons, moisture, and oxides from silicon wafers before epitaxial growth (e.g., GaN for power devices).

Quantum Computing Hardware: Eliminates surface contaminants on qubit chips (superconducting circuits/spin qubits) to prevent decoherence.

EUV Lithography Optics: Degasses multilayer mirrors to maintain reflectivity (>95%) by preventing carbon contamination.

2. Surface Science & Advanced Research

Scanning Probe Microscopy (STM/AFM): Prepares atomically clean surfaces (e.g., graphene, topological insulators) for defect-free imaging.

Molecular Beam Epitaxy (MBE): Conditions substrates (e.g., GaAs, SiC) to achieve monolayer-precision crystal growth.

Synchrotron/X-ray Experiments: Ensures sample chambers are contaminant-free to avoid beamline scattering artifacts.

3. Nuclear Fusion & Particle Physics

Tokamak Plasma Vessels: Reduces hydrogen outgassing from plasma-facing components (e.g., tungsten tiles) to stabilize fusion reactions.

Particle Accelerators: Degasses beam tubes and superconducting RF cavities to prevent electron cloud instability (e.g., in LHC/CERN).
4. Aerospace & Spacecraft Components

Optical Systems: Removes silicones/organics from telescope mirrors (e.g., James Webb) to prevent cryo-contamination.

Satellite Thruster Systems: Conditions electric propulsion components (ion thrusters) to avoid thruster poisoning.
Technical Workflow & Key Features

StepProcessPurpose
BakeoutHeating to 200–400°C under UHVDesorbs water/gases trapped in material bulk
Plasma CleaningArgon/Oxygen plasma bombardment (optional)Removes hydrocarbon films via ion sputtering
Cryo-pumpingLiquid N₂/He-cooled surfacesTraces residual gases (H₂, He, CO)
Mass SpectrometryIn-situ RGA (Residual Gas Analyzer) monitoringVerifies contamination levels at ppb/ppt scales

UHV chambers use specialized materials (stainless steel 316L, copper gaskets) and pumps (turbomolecular + ion pumps) to maintain vacuum integrity.

Critical Performance Metrics

Base Pressure: ≤5×10-10 torr (after bakeout)

Outgassing Rate: <10-12 torr·L/s·cm² (for chamber walls)

Temperature Uniformity: ±2°C across the sample (for thermal processing)

Failure Risks in UHV-Sensitive Systems

ContaminantSourceImpact
Water (H2O)Material porosityInduces hydrogen embrittlement in metals
Hydrogen (H2)Stainless steel diffusionQuenches superconductors
CO/CO2Polymer outgassingForms non-conductive layers on electrical contacts

Emerging Applications

Quantum Sensors: Degassing MEMS gravimeters/gyroscopes to reduce noise.

2D Material Synthesis: Preparing contamination-free substrates for MoS2/WSe2 growth.

Nuclear Isotope Production: Purifying targets for medical radioisotopes (e.g., ⁹⁹Mo).

Conclusion: UHV Degassing Chambers are foundational for atomic-scale manufacturing and extreme-environment systems. Unlike ASTM E595 chambers (which test material outgassing), UHV chambers actively eliminate contaminants to enable breakthroughs in quantum tech, fusion energy, and nanotechnology. For operational protocols, refer to standards like ISO 14644-7 (cleanroom compatibility) or SEMI F73 (semiconductor tool requirements).

It is a key step to improve the comprehensive capability of the discharge cavity. The amount of Desorption gas in the use of relevant parts directly affects the quality of discharge capacity, so it is necessary to establish a continuous vacuum baking degassing platform. This is mainly divided into the whole cavity baking degassing platform and parts baking degassing platform. Through the establishment of the platform, in the early stage of using the discharge chamber, a reasonable baking degassing process is established to remove the residual impurity gas and minimize the influencing factors that may affect the discharge capacity of the discharge chamber. In order to meet the above conditions, In this paper, the outline of vacuum baking platform, vacuum system, control system, heating system, special interface, other properties of the whole machine are reviewed, aiming to establish a complete vacuum baking degassing platform with full use requirements.

Diagnostics System for Plasma Characterization: Capable of providing detailed analysis of plasma parameters such as density, temperature, and potential. Tools shall include, but not limited to, Langmuir probes, Faraday cups, Residual Gas Analyzers RGA300, and Electromagnetic Spectrum Analyzer.

Cylindrical Technical Parameters:


Ultra High Vacuum Degassing Chamber

Horizontal/Vertical Chamber

Horizontal

Vertical

Model No

UHV-500

UHV-1200

UHV-3600

UHV-10000

UHV-100CBM or more

UHV-300CBM or more

Working Diameter(mm)

500

1200

1500

2000

2500~17000

3000~17000

Working Length(mm)

500

1500

2000

3000

5000~32000

6000~32000

No-load Vacuum Limit

3kPa,1kPa,10Pa133Pa0.000001Pa-0.1MPa0.001mmHg0.05Torr1*10-5Pa1*10-6Pa1*10-7Pa,1*10-9Torr,1*10-9mbar

Vacuum Limit(Option)

3kPa,1kPa,10Pa133Pa0.000001Pa-0.1MPa0.001mmHg0.05Torr1*10-5Pa1*10-6Pa1*10-7Pa,1*10-9Torr,1*10-9mbar

Temperature Range /℃

RT~3000℃

Temperature Range(Option)

RT~+150℃, 200℃, 250℃, 300℃, 400℃, 500℃, 600℃, 700℃, 800℃, 900℃, 1000℃, 1200℃, 1400℃,1600℃, 1800℃, 2000℃, 2500℃, 3000℃

Refrigerating Method

Liquid refrigerant,Refrigerating machine,Nitrogen gas temperature,Bath oil temperature, Imported compressor,Tecumseh compressor(or Bitzer Compressor),finned type evaporator,air(Water)-cooling condenser

Heating Method

SUS#304/SUS316L Stainless Steel High-speed Heater, Infrared heating array, Infrared heating cage, IR Heater

Irradiance

100W/m2~2200W/m2

Irradiation way

solar simulator,Ultraviolet irradiation simulator,Lighting environment simulation system

power conditions

AC 3Ψ 220V;3Ψ380V; 3Ψ480VNG, 60/50Hz

Customized Service

Welcome to custom size, Non-standard, Specialrequirements, OEM/ODM orders.

The technical information will be subjected to change without notice

Box Type Technical Parameters:

Model NoTUHV-500TUHV-600TUHV-800TUHV-100TUHV-2000TUHV-8000
Volume(L)125216512100020008000
Inner chamber size(mm)W*H*D 500*500*500600*600*600800*800*8001000*1000*10001200*1200*12002000*2000*2000
Temperature rangeRT+10℃~+200℃,300℃,350℃,500℃,600℃,700℃,800℃,900℃,1000℃,1200℃,1400℃,1600℃,1800℃,2000℃,2500℃,3000℃,Customization is available
Vacuum LimitVacuum Limit: 200kPa/101kPa~3kPa, 1kPa, 10Pa,133Pa,0.000001Pa,-0.1MPa,0.001mmHg,0.05Torr,1*10-5Pa,1*10-6Pa,1*10-7Pa, 1*10-9Torr, 1*10-9mbar
Final Vacuum1,No loading,≧1*10-5Pa2,Loading,≧1*10-4Pa.
PerformanceTemp fluctuation±0.5℃
Temperature UniformityAtmospheric pressure:±2℃.3Kpa Vacuum state:±50℃.(Options:±5℃,±10℃,±15℃,±30℃)
Temperature resolution0.1℃/1℃
Heating up time100℃/30min
MaterialExterior chamber material Stainless steel plate+ Power Coated
Inner chamber materialStainless steel 12X18H10T, AISI 304, AISI 316, AISI 321 or equivalentSUS#304 Stainless Steel Heater, Molybdenum / Isostatic Graphite, Infrared heating array, Infrared heating cage. 700℃ and above The Interior Chamber is 310S Stainless Steel for Vacuum Chamber, Molybdenum Heater, Molybdenum Insulation Chamber.
Insulation MaterialPU& Fiberglass wool
Feedthroughs & Flanges(Options)Custom-made feedthoughs and Options are acceptable.Drawing and Pictures for reference only. 
SystemCirculation System1.UHV Magnetic Motor & Fans(Options)2.Multi-wing centrifugal circulating fan,strengthen axis and hot cold resistance  rotary vane  make of aluminum alloy,in order to forced convection.4.FLOW THROW Air Supply Method,level diffuse vertical heat exchange arc circulation.4.Program automatic control high speed air cylinder drive high low temperature air supply valve conversion.
Heating systemSUS#304 stainless steel high-speed heater
Nitrogen systemEquipped with Nitrogen flow meter and differential pressure gauge.
Gas Analyzer(Option)Technical parameters:Measurement principle: double zirconiaDisplay mode :320x240 dot matrix color LCDMeasuring range :0-10/100/1000PPm/1.00%/25.00%02Measurement accuracy :0-1000PPm/1.00%/25.00%<+1%FS0-100PPm<+2%FS0-10PPm≤+5%FSResolution :0.1PPm(trace)0.01%(constant)Repeatability :≤+1.0%FSResponse time :Tg0≤30SOutput interface : 4-20mA. DC(non-isolated output, load resistance <1KΩ)0-10V. DC(non-high output, load resistance >10KΩ)2 programmable dry contact type passive alarm output, maximum contact capacityAC220V/2A1 channel fault alarm outputCommunication mode: RS232(Default) or RS485Power supply: AC88-264V50/60Hz, power consumption <25VAAmbient temperature: -10℃~+50℃Storage humidity: <90%BH, non-condensingWorking environment humidity: <100%RH, non-condensingSample temperature: 0℃~60℃Sampling mode: through typeSample gas flow rate: 400-600mL/minIntake pressure: 5kPa≤ relative pressure ≤200kPa(>200kPa recommended optional pressure reducing valve)Exhaust pressure: Free to empty (under safe conditions)Background gas: N2 or other inert gasSize: 145mmx175mmx301mm(HxWxD)Opening size: 135mmx135mm(HxW)Sensor life: >5 years (under normal operating conditions)Gas connection: NPT1/8 internal threadReceiving weight: Net weight 3.1KgInstallation mode: embedded Instrument features:a. Friendly man-machine dialogue menu, intuitive and convenient operation.b.320x240 graphic dot matrix color LCD display, delicate and clear display.c. The imported new type of double oxidation fault sensor has the characteristics of no power and no consumption life, high measurement accuracy, fast response speed, small zero drift and so on.d. Can work in the air for a long time, will not affect the service life of the sensor lifee. Wide measuring range, can meet the PPm~% full range test.f. Automatic temperature compensation function to reduce the impact of temperature change on the measured value.g. The instrument supports multi-point piecewise linear calibration to meet the accurate measurement of oxygen content in the full range.h. Automatic storage of 40,000 pieces of historical data, users can view historical data locally at any time.i. According to user needs, RS232(default) or RS485 data communication interface can be selected for one-way or two-way communication with the host computer. Application:It is widely used in the on-line detection and analysis of oxygen content in air separation nitrogen, smelting industry, medical and health, petrochemical industry, electronic power and other industries.Ordering Instructions (please specify when ordering)Measuring rangeThe measured gas pressureBackground gas component
Vacuum SystemGRANDE Engineering Team always configure with the Vacuum Pump as test chamber requirements of Low Pressure as below:1,Oil Sealed Vacuum Pump & Dual Stage Rotary Vane Vacuum Pump2,Roots Vacuum Pump3,Dry Vacuum Pump4,High Vacuum Pump5,Vacuum Systems-Tailored complete solutions – efficient, green and sustainable6,TURBOLAB High Vacuum Pump Systems7,Molecular Vacuum Pump8,Diffusion Pump8,Liquid Ring Vacuum Pump
Controller7Inch or 15 Inch TH5600 PID PLC ControllerPopular PID PLC controller with touch-screen operationStores 120 different profiles with up to 1200 steps each (ramp, soak, jump, auto-start, end)Step types include: ramp, soak, jump, auto-start, and endEthernet interface for remote monitoring and operationRECOMMENDED OPTIONSDry air purge, to compensate for quickly shrinking air during cooling, as well as to reduce risk of condensation.Product temperature control, allows feedback from a second sensor on the product. Ensures faster completion of transition steps.Options:Siemens or Mitsubishi PLC
Other ComponentsCable port(50mm), control status indicator lights, loading shelves(2pcs for free)
Safety protection deviceOver-heat protection circuit breaker,Control system overload protection,Overload indicator lamp.
Power SupplyAC 1Ψ 110V;AC 1Ψ 220V;3Ψ380V 60/50Hz 
Vacuum ValvesHigh-end vacuum valves, The GRANDETOP Global Service team is highly experienced and utilizes well-established, proven processes. Your goals are our #1 priority. GRANDETOP Global Service assures continuous performance improvement, minimized downtimes and ensures your vacuum equipment is running at its best performance and optimal efficiencies.Actuatorsmanual with turning handlepneumatic: single acting with closing spring (NC) or opening spring (NO), or double acting
Air Supply0.6~0.8MPa(With Self-locking fast connector)
Customized serviceWelcome to Non-standard and Specialrequirements,OEM/ODM orders.Customization of inner chamber size, tempreture&humidity range,ect.
The technical information will be subjected to change without notice